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21.
Dynamic shearing resistance of molten metal films under high pressures and extremely high shearing rates 总被引:1,自引:0,他引:1
In the present study plate-impact pressureshear experiments have been conducted to study the dynamic shearing resistance of
molten metal films at shearing rates of approximately 107 s−1. These molten films are generated by pressure-shear impact of relatively low melt-point metals such as 7075-T6 Al alloy with
high hardness and high flow-strength tool-steel plates. By employing high impact speeds and relatively smooth impacting surfaces,
normal interfacial pressures ranging from 1–3 GPa and slip speeds of over 100 m/s are generated during the pressure-shear
loading. The resulting friction stress (∼100 to 400 MPa) combined with the high slip speeds generate conditions conductive
to interfacial temperatures approaching the fully melt temperature regime of the lower melt-point metal (7075-T6 aluminum
alloy) comprising the tribo-pair.
During pressure-shear loading, laser interferometry is employed to measure normal and transverse motion at the rear surface
of the target plate. The normal component of the particle velocity provides the interfacial normal traction while the transverse
component provides the shearing resistance of the interface as it passes through melt. In order to extract the critical interfacial
parameters, such as the interfacial slip-speed and interfacial temperatures, a Lagrangian finiteelement code is developed.
The computational procedure accounts for dynamic effects, heat conduction, contact with friction, and full thermo-mechanical
coupling. At temperatures below melt the flyer and target materials are described as an isotropic thermally softening elastic-viscoplastic
solid. For material elements with temperatures in excess of the melt point, a purely Newtonian fluid constitutive model is
employed. The results of this hybrid experimental-computational study provide insights into the dynamic shearing resistance
of molten metal films at high pressures and extremely high shearing rates. 相似文献
22.
The present paper investigates the fluid–structure interaction (FSI) of a wing with two degrees of freedom (DOF), i.e., pitch and heave, in the transitional Reynolds number regime. This 2-DOF setup marks a classic configuration in aeroelasticity to demonstrate flutter stability of wings. In the past, mainly analytic approaches have been developed to investigate this challenging problem under simplifying assumptions such as potential flow. Although the classical theory offers satisfying results for certain cases, modern numerical simulations based on fully coupled approaches, which are more generally applicable and powerful, are still rarely found. Thus, the aim of this paper is to provide appropriate experimental reference data for well-defined configurations under clear operating conditions. In a follow-up contribution these will be used to demonstrate the capability of modern simulation techniques to capture instantaneous physical phenomena such as flutter. The measurements in a wind tunnel are carried out based on digital-image correlation (DIC). The investigated setup consists of a straight wing using a symmetric NACA 0012 airfoil. For the experiments the model is mounted into a frame by means of bending and torsional springs imitating the elastic behavior of the wing. Three different configurations of the wing possessing a fixed elastic axis are considered. For this purpose, the center of gravity is shifted along the chord line of the airfoil influencing the flutter stability of the setup. Still air free-oscillation tests are used to determine characteristic properties of the unloaded system (e.g. mass moment of inertia and damping ratios) for one (pitch or heave) and two degrees (pitch and heave) of freedom. The investigations on the coupled 2-DOF system in the wind tunnel are performed in an overall chord Reynolds number range of . The effect of the fluid-load induced damping is studied for the three configurations. Furthermore, the cases of limit-cycle oscillation (LCO) as well as diverging flutter motion of the wing are characterized in detail. In addition to the DIC measurements, hot-film measurements of the wake flow for the rigid and the oscillating airfoil are presented in order to distinguish effects originating from the flow and the structure. 相似文献
23.
Experimental investigation of solute transport in large,homogeneous and heterogeneous,saturated soil columns 总被引:4,自引:0,他引:4
Laboratory tracer experiments were conducted to investigate solute transport in 12.5-m long, horizontally placed soil columns during steady saturated water flow. Two columns having cross-sectional areas of 10×10cm2 were used: a uniformly packed homogeneous sandy column and a heterogeneous column containing layered, mixed, and lenticular formations of various shapes and sizes. The heterogeneous soil column gradually changed, on average, from coarse-textured at one end to fine-textured at the other end. NaCl breakthrough curves (BTC's) in the columns were measured with electrical conductivity probes inserted at 50- or 100-cm intervals. Observed BTC's in the homogeneous sandy column were relatively smooth and sigmoidal (S-shaped), while those in the heterogeneous column were very irregular, nonsigmoidal, and exhibited extensive tailing. Effective average pore-water velocities (v
eff) and dispersion coefficients (D
eff) were estimated simultaneously by fitting an analytical solution of the convection-dispersion equation to the observed BTC's. Velocity variations in the heterogeneous medium were found to be much larger than those in the homogeneous sand. Values of the dispersivity,=D
eff/v
eff, for the homogeneous sandy column ranged from 0.1 to 5.0 cm, while those for the heterogeneous column were as high as 200cm. The dispersivity for transport in both columns increased with travel distance or travel time, thus exhibiting scale-dependency. The heterogeneous soil column also showed the effects of preferential flow, i.e., some locations in the column showed earlier solute breakthrough than several locations closer to the inlet boundary. Spatial fluctuations in the dispersivity could be explained qualitatively by the particular makeup of the heterogeneities in the column. 相似文献
24.
In this work, melt spinning experiments were tentatively used for the determination of the elongational viscosity of polymer
melts at different levels of tensile strain and strain rate. The materials examined were two high-density polyethylene grades
for blow moulding with similar number-average molecular mass but different polydispersity index. The data from melt spinning
tests were compared with transient extensional viscosity data obtained by uniform isothermal tensile tests, performed by means
of an extensional rheometer, as well as with those produced by converging flow tests (Cogswell model). The results showed
that for high strain and strain rate levels, the melt spinning experiments provide elongational viscosity data quite close
to the transient extensional viscosity values obtained from the tensile tests. 相似文献
25.
This paper describes the formulation of a quasi-1-D network model, referred to as the ‘bubble model’, and its application
for simulating particle transport and filtration through a granular filter bed. The model comprises a series of homogeneous
sites linked through bundles of cylindrical bonds that represent flow pathways through distributions of pores and pore throats.
This model incorporates pore scale processes of particle sieving and infiltration are based on numerical simulations described
in a companion paper. The modeling of infiltration is further refined based on detailed experimental observations and measurements
of the filtration of a dilute suspension of acrylic particles through a column of glass beads reported by Yoon et al. (2005 Water Resour. Res., to appear). Their data distinguish (a) between the collection of particles on grain surfaces and at grain-to-grain contact
points, and (b) between particles that are fully entrapped and those that are hindered (temporarily collected) and can later
become detached. These effects are represented by two parameters that characterize the probability of attachment and are linked
to the surface roughness of the grains; one that describes the minimum particle size that can be fully entrapped, and one
that describes the detachment rate. These parameters can be readily calibrated from conventional measurements of effluent
concentration and effluent particle size distribution. Detailed comparisons with the data reported by Yoon et al. show that the proposed bubble model is able to achieve reliable predictions of the spatial distribution of particles within
the filter bed following phases of particle injection and washing. 相似文献
26.
以N,N-二甲基-1,3-丙二胺、尿素及1,4-二氯丁烷为原料,通过共缩聚反应两步法制备了一种新的主链型的水溶性聚季铵盐.采用正交试验获得了制备聚季铵盐的最佳条件:N,N-二甲基-1,3-丙二胺与尿素的物质的量比为2∶1,反应温度为135℃,反应时间为11h,得到中间体双[3-(N,N-二甲基丙胺基)]丙脲,产率高达99%;中间体与1,4-二氯丁烷的物质的量比为1∶1,于90℃下反应6h.采用红外光谱和核磁氢谱对产物结构进行表征,测定了其热稳定性和特性粘数. 相似文献
27.
28.
Madeleine A. Dallaston Christian J. Bettencourt Dr. Sharon Chow Joshua Gebhardt Jordan Spangler Dr. Martin R. Johnston Craig Wall Dr. Jason S. Brusnahan Prof. Craig M. Williams 《Chemistry (Weinheim an der Bergstrasse, Germany)》2019,25(41):9614-9618
Common oxidants used in chemical synthesis, including newly developed perruthenates, were evaluated in the context of understanding (and better appreciating) the sensitiveness and associated potential hazards of these reagents. Analysis using sealed cell differential scanning calorimetry (scDSC) facilitated Yoshida correlations, which were compared to impact sensitiveness and electrostatic discharge experiments (ESD), that enabled sensitiveness ranking. Methyltriphenylphoshonium perruthenate (MTP3, 8 ), isoamyltriphenylphosphonium perruthenate (ATP3, 7 ) and tetraphenylphosphonium perruthenate (TP3, 9 ) were found to be the most sensitive followed by 2-iodoxybenzoic acid (IBX, 2 ) and benzoyl peroxide (BPO, 10 ), whereas the most benign were observed to be Oxone ( 12 ), manganese dioxide (MnO2, 13 ), and N-bromosuccinimide (NBS, 17 ). 相似文献
29.
Emel Önal Cheng Zhang Derya Davarcı Ümit İşci Guillaume Pilet Andrew K. Whittaker Fabienne Dumoulin 《Tetrahedron letters》2018,59(6):521-523
A cyclotriphosphazene substituted with six 3,5-bis(trifluoromethyl) benzyloxy units was designed as a novel 19F MRI contrast agent. The resulting molecule has 36 magnetically equivalent fluorine atoms and exhibited suitable MRI properties with high imaging sensitivity, confirming the proof-of-concept as a convenient scaffold for the production of new 19F MRI contrasts agents. 相似文献
30.